Abstract
X-ray microtomography (XMT) has been used to characterise the microstructure and density distribution in thermally-oxidised Pile Grade A (PGA) graphite in 3-D. The needle coke filler particles can be clearly distinguished from the binder phase. Quantitative measurements of density showed that thermal oxidation occurred predominantly in the binder phase. The spatial distribution of large-scale porosity was determined. The Young’s modulus and thermal diffusivity of specimens of virgin and nominally 15% and 30% weight loss graphite were measured. It was demonstrated that weight loss calculations do not necessarily reflect the degree of oxidation and material removal throughout the bulk of the specimen. Relationships between microstructure, bulk density, and the mechanical properties were determined.
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